100029 | Acetonitrile

Acetonitrile
100029
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      Overview

      Replacement Information

      Key Spec Table

      CAS # EC Number Hill Formula Chemical Formula Molar Mass
      75-05-8200-835-2C₂H₃NCH₃CN41.05 g/mol

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      1.00029.1000
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          Glass bottle 1 l
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          1.00029.2500
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              Glass bottle 2.5 l
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              1.00029.9010
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                  Barrel stainl. st. 10 l
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                  1.00029.9030
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                      Barrel stainl. st. 30 l
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                      Description
                      Catalogue Number 100029
                      Synonyms ACN, Methyl cyanide, Ethyl nitrile, Cyanomethane
                      Overview LiChrosolv® hypergrade is accurately tested for LC-MS suitability, and meet all the requirements of modern LC-MS ionization methods (ESI/APCI - positive and negative mode). Thanks to their low level of ionic background and low ion suppression, LiChrosolv® hypergrade solvents provide high reproducibility and high ionization efficiency. The packaging material has been improved to meet LC-MS quality requirements perfectly.
                      References
                      Product Information
                      CAS number 75-05-8
                      EC index number 608-001-00-3
                      EC number 200-835-2
                      Hill Formula C₂H₃N
                      Chemical formula CH₃CN
                      Molar Mass 41.05 g/mol
                      HS Code 2926 90 95
                      Structure formula Image
                      Applications
                      Biological Information
                      Physicochemical Information
                      Boiling point 81.6 °C (1013 hPa)
                      Density 0.786 g/cm³ (20 °C)
                      Explosion limit 3.0 - 17 %(V)
                      Flash point 2 °C
                      Ignition temperature 524 °C
                      Melting Point -45.7 °C
                      Vapor pressure 97 hPa (20 °C)
                      Refractive Index 1.34
                      Solubility (20 °C) soluble
                      Dimensions
                      Materials Information
                      Toxicological Information
                      Safety Information according to GHS
                      Hazard Pictogram(s)

                      Hazard Statement(s) H225: Highly flammable liquid and vapour.
                      H302 + H312 + H332: Harmful if swallowed, in contact with skin or if inhaled
                      H319: Causes serious eye irritation.
                      Precautionary Statement(s) P210: Keep away from heat/sparks/open flames/hot surfaces. - No smoking.
                      P240: Ground/bond container and receiving equipment.
                      P302 + P352: IF ON SKIN: Wash with plenty of soap and water.
                      P305 + P351 + P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
                      P403 + P233: Store in a well-ventilated place. Keep container tightly closed.
                      Signal Word Danger
                      RTECS AL7700000
                      Storage class 3 Flammable liquids
                      WGK WGK 2 water endangering
                      Disposal 1
                      Strongly contaminated halogen-free organic solvents: container A.
                      Safety Information
                      Hazard Symbols Flammable
                      Harmful
                      Categories of danger highly flammable, harmful, irritant
                      R Phrase R 11-20/21/22-36
                      Highly flammable.Harmful by inhalation, in contact with skin and if swallowed.Irritating to eyes.
                      S Phrase S 16-36/37
                      Keep away from sources of ignition - No smoking.Wear suitable protective clothing and gloves.
                      Product Usage Statements
                      Storage and Shipping Information
                      Packaging Information
                      Transport Information
                      Declaration (railroad and road) ADR, RID UN 1648 Acetonitril, 3, II
                      Declaration (transport by air) IATA-DGR UN 1648 ACETONITRILE, 3, II
                      Declaration (transport by sea) IMDG-Code UN 1648 ACETONITRILE, 3, II
                      Supplemental Information
                      Specifications
                      Specifications
                      Purity (GC)≥ 99.9 %
                      Identity (IR)conforms
                      Evaporation residue≤ 1.0 mg/l
                      Water≤ 0.01 %
                      Colour≤ 10 Hazen
                      Acidity≤ 0.0001 meq/g
                      Alkalinity≤ 0.0002 meq/g
                      Al (Aluminium)≤ 10 ppb
                      Ca (Calcium)≤ 10 ppb
                      Fe (Iron)≤ 10 ppb
                      K (Potassium)≤ 5 ppb
                      Mg (Magnesium)≤ 10 ppb
                      Na (Sodium)≤ 50 ppb
                      Any further metal (ICP-MS)≤ 5 ppb
                      Gradient grade (at 210 nm)≤ 1.0 mAU
                      Gradient grade (at 254 nm)≤ 0.5 mAU
                      Fluorescence (as quinine at 254 nm)≤ 1.0 ppb
                      Fluorescence (as quinine at 365 nm)≤ 0.5 ppb
                      Suitability for fluorescence detection: At an excitation between 240 and 600 nm (with Δλ=10nm) the emission intensity in the range 250 - 700 nm is smaller then the following standards: quinine-standard (1ng/ml; 0,05mol/l H₂SO₄), PAH Standard (1:100000; Acetonitrile; NIST SRM 1647B)conforms
                      Transmission (at 191 nm)≥ 25 %
                      Transmission (at 195 nm)≥ 85 %
                      Transmission (at 200 nm)≥ 96 %
                      Transmission (at 215 nm)≥ 98 %
                      Transmission (from 230 nm)≥ 99 %
                      Suitability for PAH analysis: HPLC fluorescence-detectionconforms
                      Suitability for pesticide analysis: HPLC UV-detectionconforms
                      Suitable for LC-MS (tested with ion trap MS); (Intensity of background mass peak based on reserpine (APCI/ESI positiv))≤ 2 ppb
                      Suitable for LC-MS (tested with ion trap MS); Intensity of background mass peak based on reserpine (APCI/ESI negative)≤ 20 ppb
                      Filtered by 0.2 µm filter
                      Suitable for UPLC / UHPLC / Ultra HPLC - instruments
                      Suitable for Q-TOF LC-MS

                      Documentation

                      MSDS

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                      Certificates of Analysis

                      Product Number Packaging Specification Lot Number
                      1.00029.1000 Glass bottle PDF Specification Document
                      1.00029.2500 Glass bottle PDF Specification Document
                      1.00029.9010 Barrel stainl. st. PDF Specification Document
                      1.00029.9030 Barrel stainl. st. PDF Specification Document

                      Brochure

                      Title
                      UHPLC 2 - Guidelines for high throughput separations

                      Reach Use

                      Title
                      Reach Use

                      Application Notes

                      Title
                      Additives & Sweeteners in Soft drink - separation of Saccharin, Caffeine, Benzoate, Aspartame - using a Superspher RP-18 column - ion-pair method
                      Antiepileptics (Standards) - separation of 2-Ethyl-2-phenylmalonamide, Ethosuximide, Primidone, Methylpropylsuccinimide, Phenobarbital, Hexobarbital, Carbamazepine, Phenytoin - using a Purospher RP-18e column
                      Antioxidants & Preservatives (Standards) - separation of Ascorbic acid, p-Hydroxybenzoic acid, Benzoic acid, Sorbic acid, Methylparaben, Ethylparaben, Propylparaben - using a Purospher RP-18e column
                      Aromatic amines in Drinking water - separation of Aniline and selected Aniline Derivatives - using a Superspher RP-18 column with LC-MS detection
                      Chlorophylls & Xantines in Alga - separation of Pigments - using a LiChrospher RP-18e column
                      PAH (Standards) - separation of 18 PAH (16 EPA 2) - using a 250-4mm LiChrospher PAH column
                      PAH (Standards) - separation of 18 PAH (16 EPA 2) - using a 250-4mm LiChrospher PAH column - fluorescence detection
                      PAH (Standards) - separation of 18 PAH (EPA 610 2) - using a 250-3mm LiChrospher PAH column
                      PAH in Water - separation of 16 PAH's - using a LiChrospher PAH column - fluorescence detection
                      PAH in Water - separation of Fluoranthene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Benzo(a)pyrene, Benzo(ghi)perylene, Indeno(1,2,3-cd)pyrene - using a LiChrospher PAH column - fluorescence detection
                      Peak symmetry test (Standards) - separation of 4-Aminopyridine, 3-Aminopyridine, 2-Aminopyridine - using a Purospher RP-18e column
                      Pesticides (Standards) - separation of 33 Pesticides - using a Purospher RP-18e column
                      Pesticides in Drinking water - separation of 6 Triazine Herbicides, 6 Urea Herbicides, Metamitron, Chloridazon, Crimidine, Carbetamide, Bromacil, Karbutilate, Metazac - using a Superspher RP-18 column
                      Pesticides in Drinking water - separation of Dicamba, Bentazon, Dichlorprop, Mecoprop, 2-Methyl-4-chlorophenoxyacetic acid, 2-Methyl-4-chlorophenoxybutyric acid - using a LiChrospher RP select B column
                      Phenols in Water - separation of Picric acid, 2,4-Dimethylphenol, Phenol and eight Chlor- and Nitrophenols - using a LiChrospher RP select B column
                      Steroids (Standards) - separation of Benzoic acid, Sorbic acid, Cortisone - using a Purospher RP-18e column
                      Steroids (Standards) - separation of Prednisolone, Cortisone, Nortestosterone, Estradiol, Testosterone, Corticosterone, Estrone, Progesterone - using a Purospher RP-18e column

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                      Accessories (Primary)

                       Catalogue Number Description  
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                      963533 Safety carrier Show Pricing & Availability

                      Accessories (Secondary)

                       Catalogue Number Description  
                      100801 Label set acc. GHS Show Pricing & Availability
                      103830 HPLC-bottle adapter with 3 tube connections ID 3.2 mm, solvents supply Show Pricing & Availability
                      103831 HPLC bottle adapter S40 with 3 tube connections and 1 connection for exhaust air filter, solvents disposal Show Pricing & Availability
                      103833 Exhaust air filter for HPLC bottle adapter S40, disposal Show Pricing & Availability
                      108801 Bottle key Show Pricing & Availability

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                      Categories

                      Analytics and Sample Preparation > Analytical Chromatography > Mobile Phases for Chromatography > Solvents for Liquid Chromatography, LiChrosolv®
                      Reagents, Chemicals and Labware > Solvents > Solvents for Instrumental Organic Analysis > Solvents for Liquid Chromatography, LiChrosolv®