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WideScreen® Activity Assays

Activity assays are an effective and efficient way to determine the activity of your particular enzyme, the efficiency of your inhibitors or activators, or the results of upstream antagonism.  The activity assays provided by EMD are offered in a convenient plate-based set-up that allows for either manual or higher throughput analysis.
K-LISA are a subset of assays particularly tailored for the measurement of kinases from either recombinant or lysates sources.  The assay kits measure the kinase activity by utilizing a technique in which phosphorylation of a target is detected using phosphospecific antibodies of the phosphorylated protein substrates of the kinase of interest
A large number of caspases are also offered.  These assays work on the principle that caspases cleave signature peptide sequence of their targets.  When the target is cleaved, either a Fluorimetric or colorimetric substrate is released.  This allows for an easy, quantifiable detection of the caspase activity. 

When to use

  • To measure enzymatic (e.g. kinase, caspase, etc.) activity and determine the effects of activators or inhibitors.
  • The kits vary in sample compatibility, so this should be considered carefully when choosing an activity assay kit.

Advantages

  • Direct measurement of:
    • Enzymatic activity
    • Effects of inhibitors/activators

Sample Type

  • Varies – cell lysates, partially purified or purified enzyme, tissue homogenates, cell extracts

Detection

  • Colorimetric
  • Western blot

Equipment Required

  • Colorimetric ELISA plate reader
  • Western blotting equipment

 Products

Product Format Form Sensitivity Assay Range Assay Time Sample Type Cat. No.
20S Proteasome Assay Kit, SDS-Activated Cuvette or 96-well plate       30 min   539158
Calpain Activity Assay Kit, Fluorogenic 96-well plate 96 Tests     1.5 h Cell lysates, plasma, serum QIA120
Caspase-3 Activity Assay Kit, Fluorometric 96-well plate 96 Tests     2.5-3 h Cell lysates QIA70
Caspase-3 Cellular Activity Assay Kit 96-well plate 96 Tests     2.5-3 h Cell extracts 235419
Caspase-3 Detection Kit (FITC-DEVD-FMK) Flow cytometry, fluorescence microscopy 100 Tests     1.5 h Cultured cells QIA91
Caspase-3 Detection Kit (Red-DEVD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Cultured cells QIA93
Caspase-3 Inhibitor Screening Assay Kit 96-well plate 96 Tests     2 h Recombinant or purified caspase-3 235418
Caspase-3 Intracellular Activity Assay Kit II (PhiPhiLux® G2D2) Flow cytometry or fluorescence microscopy 30 Tests     1.5-2 h Intact cells 235432
Caspase-3 Intracellular Activity Assay Kit I (PhiPhiLux® G1D2) Flow cytometry or fluorescence microscopy 30 Tests     2 h Intact cells 235430
Caspase-7 Immunoassay/Activity Kit, Fluorometric 96-well plate 96 Tests     6 h Cultured cells QIA108
Caspase-8 Activity Assay Kit, Fluorometric 96-well plate 96 Tests     2-3 h Cell lysate QIA71
Caspase-8 Detection Kit (FITC-IETD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Intact cells QIA113
Caspase-8 Detection Kit (Red-IETD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Intact cells QIA114
Caspase-9 Activity Assay Kit, Fluorometric 96-well plate 96 Tests     2-3 h Cell lysate QIA72
Caspase-9 Detection Kit (FITC-LEHD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Intact cells QIA115
Caspase-9 Detection Kit (Red-LEHD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Intact cells QIA116
Caspase Detection Kit (FITC-VAD-FMK) Flow Cytometry or Fluorimeter 100 Tests     1.5 h Intact cells QIA90
Caspase Detection Kit (Red-VAD-FMK) Flow cytometry or fluorescence microscopy 100 Tests     1.5 h Intact cells QIA92
Glutathione Assay Kit Cuvette 100 Tests 5.0 µM RSH   1.5 h Cell lysates, tissue homogenates 354102
GSH/GSSG Ratio Assay Kit Cuvette 200 Tests 9 nM GSSG   1.5 h cell lysates, tissue extracts, blood 371757
JNK Activity Immunoassay Kit Immunoblot 40 Tests       Cell lysates 420115
K-LISA™ mTOR Activity Kit 96-well plate 96 Tests       Purified or partially purified enzyme CBA055
LCAT Activity Assay Kit, Fluorometric   100 Tests     4.5 - 8.5 h Plasma 428900
Nitric Oxide Assay Kit, Colorimetric 96-well plate 80 Tests     1-1.5 h Aqueous solutions 482650
Nitric Oxide Assay Kit, Fluorometric 96-well plate 192-288 Tests     3-5 h Aqueous solutions 482655
Nitric Oxide Synthase Assay Kit Scintillation vial 50 Tests picomolar range 2 h   Tissue or cell extracts 482700
Nitric Oxide Synthase Assay Kit, Colorimetric 96-well plate 96 Tests     2 h Plasma, serum, urine, tissue culture medium, and tissue homogenates 482702
OxyDNA Assay Kit, Fluorometric   50 Tests     4 h Cells 500095
Protease Assay Kit Cuvette or 96-well plate 200 Tests 10 ng/ml   3 h Biological samples 539125
PTP1B Assay Kit, Colorimetric 96-well plate 96 Tests     2 h Purified enzyme 539736
β-Secretase Activity Assay Kit, Fluorogenic Cuvette or 96-well plate 100 Tests     1.5 h Cell lysates, tissue extracts, purified BACE 565785
Superoxide Anion Detection Kit, Chemiluminescent Round-bottom polystyrene luminometer tubes 100 Tests     1.5 h Cell cultures 574590
Total Antioxidant Status Assay Kit Cuvette 50 Tests   0-25 nmol/10 µl plasma   Serum, plasma, tissue extracts, plant extracts, beverages 615700
Urokinase Activity Assay Kit, Fluorogenic 96-well plate 100 Tests 0.01 U/ml 0.78 - 50 U/ml 1.5 h Cell lysates, plasma, and serum, for screening uPA inhibitors QIA125

© Merck KGaA, Darmstadt, Germany, 2012


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