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Merck

700304

Iron oxide(II,III), magnetic nanoparticles solution

20 nm avg. part. size, 5 mg/mL in toluene

Synonyme(s) :

Magnetic iron oxide nanocrystals, Magnetite, Superparamagnetic iron oxide nanoparticles

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A propos de cet article

Formule empirique (notation de Hill) :
Fe3O4
Numéro CAS:
Poids moléculaire :
231.53
NACRES:
NA.23
PubChem Substance ID:
UNSPSC Code:
12352302
MDL number:
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Nom du produit

Iron oxide(II,III), magnetic nanoparticles solution, 20 nm avg. part. size, 5 mg/mL in toluene

InChI

1S/3Fe.4O

SMILES string

O=[Fe].O=[Fe]O[Fe]=O

InChI key

SZVJSHCCFOBDDC-UHFFFAOYSA-N

form

nanoparticles
solution

concentration

5 mg/mL in toluene

magnetization

>20 emu/g, at room temp. under 4500 Oe

avg. part. size

20 nm

particle size

20 nm (+/- 2nm TEM)

density

0.865 g/mL at 25 °C

Quality Level

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General description

Concentration 5mg/ml includes total weight nanocrystals plus ligands.

signalword

Danger

Hazard Classifications

Aquatic Chronic 3 - Asp. Tox. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 - STOT SE 3

target_organs

Central nervous system, Respiratory system

Classe de stockage

3 - Flammable liquids

wgk

WGK 3

flash_point_f

45.0 °F

flash_point_c

7.2 °C

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter


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Certificats d'analyse (COA)

Lot/Batch Number

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How do I find price and availability?

    There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

  4. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

  5. What method is used to determine the magnetization of Product 700304, Iron oxide, magnetic nanoparticles?

    A Magnetic Susceptibility Balance is used to determine the magnetic properties of this product.

  6. When using Product 700304, Iron oxide, magnetic, is it common to see particulates settle on the bottom of the bottle or would this indicate a quality problem?

    Occasionally a precipitate will form in concentrated samples, but at the 5mg/ml concentration, there should be little, if any, particulate.

  7. What is the coating thickness of oleic acid on product number 700312, 700320, and 700304, Iron oxide(II,III), magnetic nanoparticles solution?

    The suppliers of the magnetic iron oxide nanoparticles in toluene have indicated that the particles are essentially coated with a monolayer of oleic acid. Since the oleic acid is a long chain hydrocarbon there can exist some folding and irregular structure on the surface.  The suppliers estimate that one should add 1-2 nm to the particle size due to the presence of the oleic acid coating. From this, 1.5 nm is the closest approximation of coating thickness as provided by our suppliers.

  8. How should a sample of the Iron oxide(II,III), magnetic nanoparticles solution in toluene be prepared for analysis by transmission electron microscopy (TEM)?

    The particle size is determined by TEM.If the solution as provided is not diluted, a superlattice of multilayer nanocrystals will form on the grid, appearing to be an aggregate. The solution can be diluted with the same solvent that it was shipped in (toluene). A solution diluted to 0.1-0.5 mg/mL should be concentrated enough to get a nice picture. One drop per grid should be sufficient. (Since the solution is provided at a concentration of 5 mg/mL, this would be a 10- to 50-fold dilution.)After applying the sample to the grid, a drying time of a minimum of 10-15 minutes is recommended.After performing several successful dilutions and getting good results, the analyst will get a feel for the correct dilution just by judging the color and darkness of the diluted sample. If you see lone isolated dots in the TEM, then your sample is too dilute. If you cannot distinguish separate particles, it is too concentrated. Good record keeping will help to zero in on the best dilution factor for the type of picture that you want.

  9. My question is not addressed here, how can I contact Technical Service for assistance?

    Ask a Scientist here.

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