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Merck

M-108

MTBSTFA

with 1% t-BDMCS, ampule of 5 × 1 mL, analytical standard, Cerilliant®

Synonym(s):

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, N-Methyl-N-tert-butyldimethylsilyltrifluoroacetamide, MTBSTFA + 1% TBDMSCl, Silylating mixture VI

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About This Item

Empirical Formula (Hill Notation):
C9H18F3NOSi
CAS Number:
77377-52-7
Molecular Weight:
241.33
PubChem Substance ID:
329817850
UNSPSC Code:
41116107
MDL number:
MFCD00009671
Beilstein/REAXYS Number:
3606546

Product Name

MTBSTFA (with 1% t-BDMCS), ampule of 5 × 1 mL, (with 1% t-BDMCS), analytical standard, Cerilliant®

SMILES string

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI key

QRKUHYFDBWGLHJ-UHFFFAOYSA-N

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3

grade

analytical standard

reaction suitability

reagent type: derivatization reagent
reaction type: Acylations

packaging

ampule of 5 × 1 mL

manufacturer/tradename

Cerilliant®

technique(s)

gas chromatography (GC): suitable

application(s)

forensics and toxicology

format

neat

storage temp.

−20°C

Quality Level

100

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Application


  • Pharmaceutical substances in ambient particulates: A preliminary assessment.: This study explores the presence of pharmaceutical compounds in environmental particulate matter, using analytical methods that could involve derivatization agents like MTBSTFA. The detection of these substances in air samples suggests potential health impacts and environmental persistence (Cecinato et al., 2017) (Cecinato et al., 2017).


Legal Information

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany

pictograms

FlameExclamation mark
GHS02,GHS07

signalword

Warning

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Storage Class

3 - Flammable liquids

wgk

WGK 3

flash_point_f

113.0 °F - closed cup

flash_point_c

45 °C - closed cup

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Xiaowei Wang et al.
Journal of chromatography. A, 1216(35), 6267-6273 (2009-07-31)
A sample pretreatment method for the determination of 18 chlorophenols (CPs) in aqueous samples by derivatization liquid-phase microextraction (LPME) was investigated using gas chromatography-mass spectrometry. Derivatization reagent was spiked into the extraction solvent to combine derivatization and extraction into one
Martin Adiels et al.
Rapid communications in mass spectrometry : RCM, 24(5), 586-592 (2010-02-09)
Stable isotope kinetic studies play an important role in the study of very-low density lipoprotein (VLDL) metabolism, including basic and clinical research. Today, [1,1,2,3,3-(2)H(5)]glycerol is the most cost-effective alternative to measure glycerol and triglyceride kinetics. Recycling of glycerol from glycolysis
R Montes et al.
Journal of chromatography. A, 1216(2), 205-210 (2008-12-17)
A fast and novel sample preparation procedure for the determination of triclosan (TCS) and methyltriclosan (MTCS) in water samples is presented. Dispersive liquid-liquid microextraction, using a ternary mixture consisting of a disperser, an extractant and N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide (MTBSTFA) as derivatization reagent
Stephane Morville et al.
Journal of environmental monitoring : JEM, 6(12), 963-966 (2004-11-30)
A method using GC-MS and derivatization with N-(t-butyldimethylsilyl)-N-methyltrifluoroacetamide (MTBSTFA) was developed for the analysis of 20 phenolic compounds in atmospheric samples (gas and particles). Air sampling was carried out using a Hi-Vol sampler with glass fibre filter and XAD-2 resin
Ho-Sang Shin et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 879(7-8), 489-494 (2011-02-01)
A gas chromatography-mass spectrometric (GC-MS) method was developed for the determination of 2-naphthol (2-NAP) and 1-hydroxypyrene (1-HOP) in human urine. Extraction from urine after the enzyme hydrolysis with β-glucuronidase/arylsulfatase was achieved with a liquid extraction using 5 mL of pentane.
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