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KitAlysis 高通量Miyaura硼化反应筛选试剂盒-2套

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NACRES:
NA.21
UNSPSC Code:
12161600
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product line

KitAlysis

reaction suitability

reagent type: catalyst
core: palladium
reaction type: Miyaura Borylation Reaction

functional group

phosphine

General description

The KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit enables chemists to quickly and efficiently screen reaction conditions for Pd catalyzed Miyaura borylation reactions. Quick identification of optimal conditions allows faster scale-up of the desired synthetic transformation. All required chemicals come pre-weighed for ease of use. A step-by-step user guide and experimental excel sheets are available for download to facilitate the process.

Application

Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:

  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC


试剂盒组分也可单独购买

产品编号
说明
化学品安全说明书 & 价格

  • P(Cy3) Pd G3, 97%
    化学品安全说明书

  • Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%
    化学品安全说明书

  • XPhos Pd G4, 95%
    化学品安全说明书

  • SPhos Pd G4
    化学品安全说明书

  • RuPhos Pd G4
    化学品安全说明书

  • DTBPF-Pd-G3
    化学品安全说明书

  • cataCXium A Pd G4
    化学品安全说明书

查看所有结果 (21)

signalword

Danger

target_organs

Central nervous system, Eyes,Central nervous system, Kidney, Respiratory system

supp_hazards

存储类别

3 - Flammable liquids

flash_point_f

1.4 °F

flash_point_c

-17 °C

wgk

WGK 3

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT RE 2 Oral - STOT SE 1 - STOT SE 3



历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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实验方案

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

商品

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

KitAlysis High-Throughput Screening Kits enable efficient identification and optimization of catalytic reaction conditions.

相关内容

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

有机合成中的化学反应设计和优化旨在精确改变反应参数,以达到最佳效果,找到通向目标分子的途径。

查看所有相关内容