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Merck

395056

Methylamine solution

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2.0 M in THF

Synonym(s):

Monomethylamine

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About This Item

Linear Formula:
CH3NH2
CAS Number:
74-89-5
Molecular Weight:
31.06
UNSPSC Code:
12352302
NACRES:
NA.22
PubChem Substance ID:
57649902
MDL number:
MFCD00008104
Beilstein/REAXYS Number:
741851

Product Name

Methylamine solution, 2.0 M in THF

InChI

1S/CH5N/c1-2/h2H2,1H3

SMILES string

CN

InChI key

BAVYZALUXZFZLV-UHFFFAOYSA-N

vapor pressure

23.87 psi ( 55 °C)
7.24 psi ( 20 °C)

form

liquid

greener alternative product characteristics

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concentration

2.0 M in THF

density

0.861 g/mL at 25 °C

functional group

amine

greener alternative category

Enabling,

Quality Level

200

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Application

Methylamine can be used as a reagent in the synthesis of the following:     
  • Methylmorpholine from diethylene glycol.       
  • N-methylalkylamines from oxoamines via formation of imine, followed by hydrogenation using Ni catalyst.   
  • N-Methyldipropylenetriamine by reacting with acrylonitrile, followed by hydrogenation.  
  • N-methyl hydroxypyrrolidines from chlorohydrin in the presence of NaCNBH as a reducing agent.       
  • 2-(Methylamino)-6,7-dichloro-1,4-anthracenedione by reacting with 6,7-dichloro-1,4-anthracenedione.

Methylamine solution 2.0 M in THF can be used as a precursor that facilitates the synthesis of perovskite based materials. It can also be used as a deactivating agent to study the catalytic performance of acidic macroporous ion exchange resins. It can be annealed to reduce impurity in the grain boundaries, improve the stability and efficiency of the perovskite solar cells.

General description

Methylamine (CH3NH2) is a simple aliphatic primary amine used as a chemical intermediate in organic synthesis. It is prominently used in the production of pesticides and solvents.
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Danger

Hazard Classifications

Acute Tox. 4 Oral - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1B - STOT SE 3

target_organs

Respiratory system

supp_hazards

EUH019

Storage Class

3 - Flammable liquids

wgk

WGK 1

flash_point_f

<-29.2 °F - closed cup

flash_point_c

< -34 °C - closed cup

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

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Certificates of Analysis (COA)

Lot/Batch Number
MKCZ9455
BCCN1600
MKCW4805
BCCM2139
BCCH9267

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Jason A Draper et al.
Organic letters, 12(18), 4034-4037 (2010-08-24)
A convergent and stereoselective synthesis of 2,5-disubstituted 3-hydroxypyrrolidines has been developed that involves reductive annulation of β-iminochlorohydrins, which are readily available from β-ketochlorohydrins, and provides rapid access to a variety of 2,5-syn-pyrrolidines. Application of this process to the concise (three-step)
Amines, aliphatic
Eller K, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2000)
Synthesis and in vitro antitumor activity of substituted anthracene-1, 4-diones
Hua DH, et al.
Tetrahedron, 60(45), 10155-10163 (2004)
Methylamines synthesis: A review
Corbin DR, et al.
Catalysis Today, 37(2), 71-102 (1997)
Deactivation of ion exchange catalysts by acetonitrile and methylamine
Gonzalez R, et al.
Topics in Catalysis, 54(16-18), 1054-1054 (2011)
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