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Merck

KITALYSIS-24PD

KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2

别名:

Pd Precatalysts

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关于此项目

NACRES:
NA.22
UNSPSC Code:
12161600
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product line

KitAlysis

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction, reaction type: Heck Reaction, reaction type: Hiyama Coupling, reaction type: Negishi Coupling, reaction type: Sonogashira Coupling, reaction type: Stille Coupling, reaction type: Suzuki-Miyaura Coupling, reagent type: catalyst
reaction type: Cross Couplings

functional group

phosphine

Application

Screening kit for cross-coupling reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

Downloadable experimental Excel Sheet

Each kit contains 2 customizable screening sets that include the following components:

  • 24 pre-weighed catalysts in glass micro vials loaded with stir bars and topped with cap mat.
  • 2 KitAlysis 24-Well reaction block replacement films.
  • 4 empty substrate stock solution reaction vials with stir bars.
  • 3 stir bars for stock solutions.
  • 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
  • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC


signalword

Warning

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - Skin Sens. 1 - STOT SE 3

target_organs

Respiratory system

supp_hazards

存储类别

10 - Combustible liquids

flash_point_f

Not applicable

flash_point_c

Not applicable

wgk

WGK 3



历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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实验方案

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

商品

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

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相关内容

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

有机合成中的化学反应设计和优化旨在精确改变反应参数,以达到最佳效果,找到通向目标分子的途径。

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